For reliable and reproducible results from fracture testing, some basic rules must be taken into consideration.
Biological
materials are notoriously variable in their morphology and structure.
Variation can occur not only at any or all of the hierarchical levels
from the molecular, through to material and structural level, but also
within the entire test specimen and even between specimens.
Wedge
penetration, a type of crack opening test that is particularly
suitable to testing fruit and vegetables, cheese, stiff gels and cooked
meats, involves a wedge driven into a block of material.
The
dimensions of the test specimen affect the results and so it is
important to use reproducible rectangular blocks. This test is similar
to a tensile test but instead of the two halves of the specimen being
pulled, they are pushed out by the penetrating wedge. The two halves
bend outward storing strain energy.
At
the point of fracture this energy is fed to the tip of the wedge where
stress concentration is highest and a free running crack starts and
propagates ahead of the wedge.
This
is a versatile test and can be applied to many types of products that
are available in, or can be cut or shaped into, elongated test beams.
The
most conventional method is a three-point bend test in which the
specimen is supported horizontally at either end like a bridge and a
probe moving downwards bends it in the centre. As the specimen bends it
stores up strain energy, which is dissipated in cracking at the point of
fracture.
Compression tests can be carried out on a wide variety of products that experience such a force in natural conditions.
These
may include fruit and vegetables, puffed cereals, cakes and biscuits,
confectionery and pharmaceuticals.
Normally, as these products may be oddly
shaped, a compressive test is the most reliable way of assessing their
fracture behaviour.
Many
foods and pharmaceuticals are not normally subject to tensile forces in
their manufacture and consumption. There are, however, exceptions, e.g.
dough, gels, spaghetti and adhesives.
These
tests can also be performed on materials from which elongated test
specimens can be cut and gripped within the clamps of the Texture
Analyser to be stretched. This could include fruit, vegetables and meat.
In any case this type of test yields reliable results for tensile
modulus, yield stress and strain, strength and strain to fracture, and,
if the crack area can be measured, the fracture toughness of the
material.
Fracture
is simply crack propagation. Force has to be exerted to initiate a
crack, then energy has to be supplied to propagate it. This is the
energy that goes into breaking the bonds within the material in order to
generate new surfaces.
There
are three ways a crack can propagate within a material. All structural
failures are the result of material failure in one of these three modes.
What
is Fracture? This is the first of a set of blog posts on the subject of
fracture testing. Traditional information on fracture testing focusses
on techniques for assessing engineering materials using standard methods
and strict geometries. However, these may not be so useful for the
typical user of a Texture Analyser.
The loosest definition of fracture is “a form of failure in which the material separates into two or more pieces due to an applied load”.
Fracture strength is the stress at which a specimen fails or fractures.
Fracture can be brittle, ductile or semi-ductile. This refers to the
nature of deformation and will be covered in the next post.